TVSM-3000 Vibrating Sample Magnetometer

Short Description:

TVSM-3000 Vibrating Sample MagnetometerProfile ■ Hysteresis line (M-H) can be te...


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TVSM-3000 Vibrating Sample Magnetometer


Profile 

■ Hysteresis line (M-H) can be tested, coercivity, residual magnetization strength and saturation moment parameters can be obtained.

■ Testing of magnetic moment temperature curve (M-T), superconducting transition temperature (with low-temperature option), Curie temperature point (with high-temperature option).

■ 360° continuous motorized rotation of the vibration head is standard.

■ Sample auto-centering design for high accuracy and repeatability.


Vibratinga Smple Magnetometer

(Auto-alignment software interface)

■ Continuous acquisition of magnetic moment, magnetic field and temperature values at 10ms intervals

■ Electromagnet magnetic field changes at rates up to 5000 Oe/s, with hysteresis loops obtained in as little as 14s.

■ 10mm amplitude for a long period of time (24 hours) of five parts per million (5μm) stability can be achieved

■ Support for vector magnetic moment testing (optional)

■ Integrated design of the magnetic moment signal acquisition coil and Gaussmeter probe.


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Functions and Features


  • The hysteresis loop (M-H) can be tested, and the parameters such as coercivity, residual magnetization and saturation magnetic moment can be obtained;
  • Can test the magnetic moment temperature curve (M-T), with the low temperature option can get the superconducting transition temperature, with the high temperature option can get the Curie temperature point;
  • System comes standard with a vibrating head with 360 ° continuous electric rotation, and the sample is in the center of the acquisition coil and magnetic field during continuous rotation. Compared with VSM in the form of superconducting magnet,is more convenient for the study of anisotropy;
  • Specially designed electromagnet magnetic field gap adjustment method to ensure that the sample rod no longer needs to adjust the center in the left and right directions; Extremely precise mechanical devices ensure that the sample rod is at the center of the front and rear directions of the collection coil every time; The new concept of electric lifting system can automatically complete the adjustment of the sample center position in the up and down direction; The above three aspects of design can greatly improve the accuracy and repeatability of the test;
  • Test speed has been revolutionarily accelerated, and the magnetic moment, magnetic field and temperature values can be continuously collected at intervals of 10ms to ensure that users can capture any details of rapid changes in the test process. The change rate of electromagnet magnetic field is as high as 5000 Oe/s, which is a rate that superconducting magnets cannot have. At this high-speed magnetic field change rate and high-speed data acquisition rate, a hysteresis loop can be obtained in 14s;
  • Introduces a high-precision laser displacement sensor, which can distinguish the amplitude change of 1 micron, and forms a closed-loop control with a special customized sample vibration drive system, which can achieve a stability of 5/10000 for a long time (24 hours) of 10mm amplitude;
  • The option replacement and alignment device with comprehensive design to ensure that the sample vibrates up and down perpendicular to the ground without "hitting the wall" when using all options. Vector magnetic moment test is also supported for high and low temperature options;
  • Magnetic moment signal acquisition coil and gauss meter probe are integrated, occupying less space, more convenient installation, and more reliable cables;
  • Has a patented appearance design, the ease of operation of replacing samples with one hand, and the human-computer interaction interface of one-key software testing.
  • Material to be measured:
  • Diamagnetic, paramagnetic, ferromagnetic, antiferromagnetic and anisotropic materials granular and continuous magnetic recording materials and GMR, CMR, exchange bias and spin valve materials

  • Magnetic optical materials Bulk materials, powders, films, single crystals and easy-to-hold liquids


Specifications and Parameters

 

 

Magnetic Field Parameters

 

Sample Temperature

Air gap between pole heads

Sample Area

9005

9007

Room Temperature

7.5mm

3.5mm

2.78T

3.01

12mm

8mm

2.55T

2.75

High and Low Temperature

20mm

8mm

1.30

2.36

28mm

8mm

1.10

2.02

Magnetic Field Performance

Sample lifting rotation

Accuracy

1%

lifting accuracy

0.1mm

Resolution

1 mOe

Lifting range

0 to 300mm

Repeatability

100 mOe

Rotation range

0 to 730°

rotation accuracy

0.1 °

 

 

 

Magnetic Moment Measurement

 

Noise

0.1s/pt(RMS)

0.1s/pt(P-P)

1s/pt(RMS)

1s/pt(P-P)

10s/pt(RMS)

10s/pt(P-P)

Room Temperature(@3.5mm)

150 nemu

800nemu

80 nemu

380nemu

40nemu

80nemu

High Temperature or Low Temperature(@ 8mm)

0.5μemu

2.5μemu

TBD

TBD

0.1μemu

0.2μemu

Dynamic range

35*10-9emu to 103emu

Sensitivity

1x10-7emu

Time Constant

0.03s, 0.1s, 0.3s, 1.0s, 3.0s, or 10.0s

Stability

±0.05% of full scale/day

conditions:fixed coil spacing under constant temperature and magnetic fieldrelativemaximum range and requires2hour heat balance24hours of measured data.

Repeatability

± 0.5%

conditions:the same coil spacing, repeat loading and removing the sample ten times at the same rangeMeasured.

Accuracy

± 1%(contrastNIST 772astandard sample)

Sample Quality

0 to 10g

Note:of a larger mass sample leads to a decrease in amplitude resulting in a lower signal-to-noise ratio.

Other parameters

system sampling frequency0.01~10s(continuous mode10ms);

lock-in amplifier time constant is fixed100ms, low-pass steep drop18dB/oct;

vibration amplitude5 ~10mm(default8mm), vibration frequency55~85Hz(default57Hz).


sample rod

 

TVSM-3000 Vibrating Sample Magnetometer(图2)TVSM-3000 Vibrating Sample Magnetometer(图3)

 

 

Room temperature and low temperature sample rod(glass fiber)

 

Part Number

can be loaded with samples

Sample Cup Material

Maximum sample space (mm)

90001

block

acrylic

Φ4*10

90002

powder

acrylic, disposable

Φ4*10

90003

film, out-of-plane

acrylic

10*6.4

90003m

film, out-of-plane

acrylic, small

10*2.5

90004

film, in-plane

acrylic

6.4*10 (6.4*6.4 with thermostat)

90004m

film, in-plane

acrylic, small

2.5*10 (2.5*5 with thermostat)

90005

liquid

acrylic, sealed O ring

Φ2.5*7.5

TVSM-3000 Vibrating Sample Magnetometer(图4)

TVSM-3000 Vibrating Sample Magnetometer(图5)90001 90002

TVSM-3000 Vibrating Sample Magnetometer(图6)TVSM-3000 Vibrating Sample Magnetometer(图7)

 

90003 90003m

TVSM-3000 Vibrating Sample Magnetometer(图8)TVSM-3000 Vibrating Sample Magnetometer(图9)

 

 

 

TVSM-3000 Vibrating Sample Magnetometer(图10)

90004 90004m

TVSM-3000 Vibrating Sample Magnetometer(图11)TVSM-3000 Vibrating Sample Magnetometer(图12)

 

90005

TVSM-3000 Vibrating Sample Magnetometer(图13)

 

 

 

High Temperature Sample Rod (Quartz) 

Number

can be loaded with samples

Sample Cup Material

Maximum sample space (mm)

90011

block and powder

boron nitride, disposable when filling powder

Φ4*10

90012

film, out-of-plane

boron nitride

13*6

90013

film, in-plane

boron nitride

6.4*6.4

 

90011

TVSM-3000 Vibrating Sample Magnetometer(图14)

90012

TVSM-3000 Vibrating Sample Magnetometer(图15)

90013

TVSM-3000 Vibrating Sample Magnetometer(图16)

 

 

 

Temperature Range 

High Temperature Range

80K-350K

Low  Temperature

RT-1000K

 

Cryostat

TVSM-3000 Vibrating Sample Magnetometer(图17)TVSM-3000 Vibrating Sample Magnetometer(图18)

 

High temperature furnace

TVSM-3000 Vibrating Sample Magnetometer(图19)


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